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A copper-catalyzed one-pot synthesis of novel 2,3-diarylisoindole derivatives is described. The coupling reaction of phenylboronic acid, an aryl halide, and isoquinoline N-oxide (INO) or isoquinoline-5-sulfonamide (IQ5SA) is achieved with copper acetate in the presence of an iodinating agent. 2-Arylisoindole derivatives, which are obtained from an aryl halide and INO, are efficiently transformed to the corresponding 3-arylisoindole derivatives by eliminating aryl halides or arylboronic acids with acid. The presence of quinazolin-4-one moieties in the substrates was utilized to yield 3-arylisoquinoline derivatives in high yield from an INO or IQ5SA and the resulting arylboronic acid or arylboronic acid in situ.[Dynamics of hyperthermic pulmonary oedema in dogs. Effect of diuretics and alkalosis].
In this experiment a total of 26 anaesthetized dogs were subjected to thermal stress over a period of 8 hours. We observed a marked hyperthermic pulmonary oedema (HPO) after 1 hour lasting for 6 hours (0.1 mg/kg/min) with increasing pulmonary hypertension and cardiac output. An addition of 5 mg/kg/min furosemide (FD) with or without 5
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